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3  WATER CONTENT DETERMINATION




               3.1  Experiment outcomes
                           Determine the mass of soil solids.
                           Determine the mass of pore water.
                           Determine the water (moisture) content of soils



               3.2  Theory

                      The soil moisture content may be expressed by weight as the ratio of the

                      mass of water present to the dry to the dry weight of the soil sample, or by
                      volume as ratio of volume of water to the total volume of the soil sample. To
                      determine any of these ratios for a particular soil sample, the water mass

                      must be determined by drying the soil to constant weight and measuring the
                      soil sample mass after and before drying. The water mass (or weight) is the

                      difference  between  the  weights  of  the  wet  and  oven  dry  samples.  The
                      criterion  for  a  dry  soil  sample  is  the  soil  sample  that  has  been  dried  to

                                                                                               o
                                                                                                       o
                      constant  weight  in  oven  at  temperature  between  100  –  110 C  (105 C  is
                      typical).  It  seems  that  this  temperature  range  has  been  based  on  water
                      boiling temperature and does not consider the soil physical and chemical
                      characteristics.


                      Water content determination by the gravimetric method involves collecting

                      and  weighing  a  moist  sample,  removing  the  water  by  oven  drying,  and
                      weighing the dry sample. Water content is determined by calculation.
                      Two factors are important in this simple process. First, the sample must not

                      be allowed to lose water between collection and weighing. This implies use
                      of an air tight sample collection can (taped closed if storage time will be more

                      than a few hours) and weighing as soon as possible after collection. Plastic
                      bags, which are somewhat permeable  to air, should be used only if storage

                      time will be short and high accuracy is not critical.


                      Second,  a  "standard"  dryness  must  be  reached.  Some  water  (called
                                                                                                      o
                      hygroscopic or molecular) is held by soil even after drying at above 100 C for
                      several days. However, high temperatures will oxidize the organic matter.

                                                      0
                      Consequently, drying at 105 C until a constant mass is attained (usually less

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